One and Two Dimensional NMR Spectroscopy

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Decoupling Experiments -- 6. Altering the Chemical Structure of the Sample -- 6.


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Effects of Solvent and Temperature -- 6. Shift Reagents -- 6. Chiral Lanthanide Shift Reagents -- 6. Alkanes -- 6. T1 Measurements -- 6. Chemical Changes to the Sample -- 6. Solvent and Temperature Effects and Shift Reagents -- 6. Searching for Identical or Related Compounds -- 6. Spectrum Prediction -- Exercises -- 6. Bibliography for Chapter 6 -- 7. Introduction -- 7. Relaxation Mechanisms -- 7.

Relationships between T1 and Chemical Structure -- 7.

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Influence of Molecular Size -- 7. Segmental Mobilities -- 7. Anisotropy of the Molecular Mobility -- 7. Suppression of the Water Signal -- 7. Spin-Spin Relaxation T2 -- 7. Bibliography for Chapter 7 -- 8. Introduction -- 8.

By Horst Friebolin Basic One and Two Dimensional NMR Spectroscopy 4th fourth Edition Pdf

Spin-Locking -- 8. Signal Enhancement by Polarization Transfer -- 8. The SPI Experiment -- 8. Bibliography for Chapter 8 -- 9. Introduction -- 9. Preparation, Evolution and Mixing, Data Acquisition -- 9. Graphical Representation -- 9.

Basic One- and Two-Dimensional NMR Spectroscopy : Horst Friebolin :

Summary of Chapters 8 and 9 -- Exercises -- 9. Bibliography for Chapter 9 -- The Nuclear Overhauser Effect -- Introduction -- Theoretical Background -- The Two-Spin System -- Enhancement Factors -- Multi-Spin Systems -- Experimental Aspects -- Applications -- Exercises. Note continued: Bibliography for Chapter 10 -- Quantitative Calculations -- Complete Line-shape Analysis -- Activation Parameters -- Estimating the Limits of Error -- Rate Constants in Reactions with Intermediate Stages -- Intermolecular Exchange Processes -- Applications -- Rotation about CC Single Bonds -- C sp3 -C sp3 Bonds -- C sp2 -C sp3 Bonds -- C sp2 -C sp2 Bonds -- Rotation about a Partial Double Bond.

Inversion at Nitrogen and Phosphorus Atoms -- Ring Inversion -- Valence Tautomerism -- Keto-Enol Tautomerism -- Intermolecular Proton Exchange -- Reactions and Equilibration Processes -- Exercises -- Bibliography for Chapter 11 -- Synthetic Polymers -- The Tacticity of Polymers -- Polymerization of Dienes -- Copolymers -- Bibliography for Chapter 12 -- Elucidating Reaction Pathways in Biochemistry -- Syntheses using Singly 13C-Labeled Precursors -- Low Levels of 13C Enrichment -- High Levels of 13C Enrichment -- Syntheses using Doubly 13C-Labeled Precursors.

Basic one- and two-dimensional NMR spectroscopy

Biopolymers -- Peptides and Proteins -- Sequence Analysis -- The Three-Dimensional Structure of Proteins -- Polynucleotides -- Oligosaccharides and Polysaccharides -- Bibliography for Chapter 13 -- The Problem and its Solution -- Magnetic Resonance Tomography -- Basic Principles and Experimental Considerations -- David R. Glenn et al. High-resolution magnetic resonance spectroscopy using a solid-state spin sensor, Nature This document is subject to copyright.

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Basic One & Two Dimensional Nmr Spectroscopy

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